东北大学学报(自然科学版) ›› 2007, Vol. 28 ›› Issue (9): 1365-1368.DOI: -

• 论著 • 上一篇    

共轭双滑移取向铜单晶疲劳位错结构的SEM-ECC观察

李小武;周杨;杨瑞青;苏会和;   

  1. 东北大学理学院;东北大学理学院;中国科学院金属研究所;中国科学院金属研究所 辽宁沈阳110004;辽宁沈阳110004;辽宁沈阳110016;辽宁沈阳110016
  • 收稿日期:2013-06-24 修回日期:2013-06-24 出版日期:2007-09-15 发布日期:2013-06-24
  • 通讯作者: Li, X.-W.
  • 作者简介:-
  • 基金资助:
    国家自然科学基金资助项目(50671023);;

SEM-ECC observations of dislocation structures in fatigued copper single crystals oriented for conjugate double slip

Li, Xiao-Wu (1); Zhou, Yang (1); Yang, Rui-Qing (2); Su, Hui-He (2)   

  1. (1) School of Sciences, Northeastern University, Shenyang 110004, China; (2) Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
  • Received:2013-06-24 Revised:2013-06-24 Online:2007-09-15 Published:2013-06-24
  • Contact: Li, X.-W.
  • About author:-
  • Supported by:
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摘要: 利用扫描电镜电子通道衬度(SEM-ECC)技术观察和分析了[■ 2 3]和[■ 1 2]共轭双滑移取向铜单晶体的循环饱和位错结构.结果表明,驻留滑移带(PSBs)的位错结构随晶体取向的不同可呈现出不同的形态,如:[■ 1 2]晶体中的楼梯结构和[■ 2 3]晶体中的沿主滑移面排列的不规则或较规则胞结构.同时还观察到[■ 2 3]晶体中形变带的位错结构由一些不规则的墙和胞结构组成.对于晶体取向位于标准取向三角形[0 0 1]-[■ 1 1]边上的铜单晶体,其疲劳位错结构随晶体取向的不同发生有规律的变化,即:当晶体取向从[■ 1 2]分别向[■ 1 1]和[0 0 1]移动时,位错结构由PSB楼梯...

关键词: 铜单晶, 共轭双滑移, 循环形变, 位错结构, SEM-ECC技术, 晶体取向

Abstract: The dislocation structures in cyclically saturated copper single crystals oriented towards [2¯23] and [1¯12] conjugate double slip were observed and analyzed using electron-channelling contrast technique in scanning electron microscopy (SEM-ECC). It was found that the persistent slip bands (PSBs) might exhibit different dislocation features depending upon crystallographic orientation, such as ladder structures in the [1¯12] crystal and irregular or partially regular cell structures aligned along the primary slip plane in the [2¯23] crystal. Moreover, the dislocation microstructures in deformation bands (DBs) formed in the [2¯23] crystal were observed comprising irregular dislocation walls and cells. For the crystals located on the [001]-[1¯11] side of the standard stereographic triangle, the dislocation structures change regularly with the variation in crystallographic orientation. When the orientation varies from the [1¯12] orientation to [1¯11] or [001], the dislocation structures would evolve from PSB ladders as cells or labyrinths.

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