东北大学学报（自然科学版）

东北大学学报(自然科学版) ›› 2005, Vol. 26 ›› Issue (11): 79-81.DOI: -

• 论著 • 上一篇    下一篇

氧化锌棒晶的热液制备与表征

张艳辉;田彦文;邵忠财;钱建华   

  1. 东北大学材料与冶金学院;东北大学材料与冶金学院;沈阳理工大学环境与化学工程学院;渤海大学化学化工学院 辽宁沈阳110004
  • 收稿日期:2013-06-24 修回日期:2013-06-24 出版日期:2005-11-15 发布日期:2013-06-24
  • 通讯作者: Zhang, Y.-H.
  • 作者简介:-
  • 基金资助:
    国家自然科学基金资助项目(50174015)

Hydrothermal synthesis and characterization of ZnO rod-like crystal

Zhang, Yan-Hui (1); Tian, Yan-Wen (1); Shao, Zhong-Cai (2); Qian, Jian-Hua (3)   

  1. (1) School of Materials and Metallurgy, Northeastern University, Shenyang 110004, China; (2) Faculty of Environment and Chemical Engineering, Shenyang Ligong University, Shenyang 110168, China; (3) Faculty of Chemistry and Chemical Engineering, Bohai University, Jinzhou 121000, China
  • Received:2013-06-24 Revised:2013-06-24 Online:2005-11-15 Published:2013-06-24
  • Contact: Zhang, Y.-H.
  • About author:-
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摘要： 以二水醋酸锌、氢氧化钠为原料,长链聚乙二醇(PEG-20000)、环己烷为添加剂,制备出氧化锌微晶粉体.采用X射线衍射,扫描电镜和透射电镜等分析手段对粉体进行了表征.实验结果表明,在热液环境中,利用长链PEG不仅可以制备特殊形貌的氧化锌,也可以在环己烷的作用下,制备出大长径比的一维氧化锌棒.

关键词: 氧化锌, 棒晶, PEG, 环己烷, 水热法

Abstract: Zn(Ac)2 · 2H2O and NaOH were used as experimental material to synthesize ZnO microcrystal powder with long-chain PEG and cyclohexane as additives. XRD, SEM and TEM were used to characterize the powder. The experimental results showed that not only the special shape of ZnO was produced under the action of long-chain PEG, but also the one-dimension of rod-like ZnO with big aspect ratio can also be produced under the action of cyclohexane.

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