New Method for Measuring Additives in TinPlating Solution

doi:10.12068/j.issn.1005-3026.2014.10.015

Abstract

Abstract: A high performance liquid chromatographic (HPLC) method was established for the analysis of αnaphthol polyoxyethylene ether and αnaphtha sulfonate polyoxyethylene ether in tinplating solution. Plating solution was first treated with sodium phosphate dibasic to detach Sn2+ and Fe2+. The extracts were then cleanedup by high performance liquid chromatography with an ultraviolet detector on a Agilent ZORBAX Eclipse XDBC18 column by UV at 215 nm， using 20 mmol/L sodium phosphatemethanol (48∶52) as a mobile phase. The average recoveries of this method were in the range of 966%~989%. The deviation of HPLC was less than 005 g/L.The proposed method was fast， accurate， sensitive， reproducible， and it could meet the requirement of tinplating process.

Key words: HPLC, tinplating solution, additive, sodium phosphate dibasic, tinplating process

CLC Number:

TQ1531

LI Binghu， LIU Changsheng， TANG Gangfeng， JIA Yu. New Method for Measuring Additives in TinPlating Solution[J]. Journal of Northeastern University Natural Science, 2014, 35(10): 1432-1436.

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